Large-scale synthesis of per-O-acetylated saccharides and their sequential transformation to glycosyl bromides and thioglycosides

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题名:	Large-scale synthesis of per-O-acetylated saccharides and their sequential transformation to glycosyl bromides and thioglycosides
作者:	Lin, Chang-Ching Huang, Li-Cheng Liang, Pi-Hui Liu, Ching-Yang Lin, Chun-Cheng
贡献者:	化學系
关键词:	acetylation LiClO4 one-pot synthesis glycosyl bromides thioglycosides
日期:	2006
上传时间:	2009-11-20 13:25:03 (UTC+8)
摘要:	This work describes a large-scale synthesis of per-O-acetylated mono- and disaccharides using a stoichiometric amount of acetic anhydride in the presence of LiClO4 under solvent-free conditions. The peracetylated saccharides underwent subsequent anomeric bromination and thioglycosidation in one-pot to yield synthetically valuable building blocks.
關聯:	JOURNAL OF CARBOHYDRATE CHEMISTRY Volume: 25 Issue: 4 Pages: 303-313
显示于类别:	[化學系所] 期刊論文

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